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.Fiber Quality Analyzer - 360 (FQA-360) - OpTest

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.Fiber Quality Analyzer - 360 (FQA-360)

The FQA rapidly and accurately measures fiber length, width, curl, % numeric fines, and kink in dilute pulp samples. Optional software is available to measure mean fiber coarseness according to ISO 23713, Fiber Wall Thickness, hardwood/softwood blends, Degree of External Fiber Fibrillation, analyze shives and analyze vessel elements. The patented flow cell resists plugging or fouling and orients fibers for correct image analysis. The FQA meets or exceeds the specification of Tappi Test Method T271, PAPTAC B.4 and ISO 16065-1 and -2.  Accessories include the 6 Beaker Carousel and OpTiBlend software.

Product Name Fiber Quality Analyzer - 360 (FQA-360)
Product Code LDA17
Standards/Methods TAPPI T 271, ISO 16065-1, ISO 16065-2, ISO 23713, PAPTAC B.4
Test Material Pulp
Manufacturer OpTest Equipment Inc.
Availability from OpTest Worldwide

The FQA-360 features a flow cell that stays clean and does not plug. It easily measures difficult pulps without special pre-treatment or screening.

 

These pulps include:

• High Shive Content Pulps
• Mechanical Pulps
• Linerboard Pulps
• Diaper Fluff and Pulps with High Flocculation Propensity
• Recycled Fibers
• Non-wood (plant) Fibers and Long Synthetic (birefringent) Fibers

 

The 3mm rayon fibers above have no fines. However, air bubbles in the non-polarized part appear as fines

fines

The same cellulose fiber viewed with circular polarized light (left) and linear polarized light (right). The ends of the curled fiber disappear in linear polarized light.

circular or linear

• Rapid & accurate measurement of length, width, curl & kink on fibers up to 15 mm
• All fiber values are measured simultaneously with a single camera
• Combined fiber length and width data provides a useful tool for pulp blending
• Circular polarized light provides the most accurate measurement of fiber length and shape
• Sample cleaning and de-airing are unnecessary, unlike many non-polarized light methods
• More precise than non-polarized light methods
• The patented cytometric flow cell stays clean and prevents plugging
• Characterize pulps with contaminants such as ink, fillers, extractives and pitch
• Exceeds the Standard Specifications of Tappi T271, PAPTAC B.4, and ISO 16065-1
• Minimal maintenance

flowcell

 

FQA-360 Software Options

 

COARSENESS, FIBER WALL THICKNESS AND HARDWOOD/SOFTWOOD RATIO MIXTURE SOFTWARE

 

Coarseness: This option allows the FQA-360, and HiRes FQA, to accurately measure the mean fiber coarseness of a pulp sample.
The mean fiber coarseness is defined as:
coarseness = (OD sample mass) / (total fiber length)
Published results [Olson et al, Tappi J. (Oct. 1999)] found that the FQA agreed significantly with standard microscopy.
Coarseness accuracy with the FQA is ensured because the entire sample is drawn from the beaker eliminating errors from poor mixing or fiber flow fractionation.
The FQA-360 Coarseness measurement meets all the requirements and specifications of ISO Standard 23713.

coarseness

Hwd/Swd Ratio: The software prompts the user to enter the average fiber length, Lw, and coarseness, C, of the parent species. It uses these values to estimate the fraction, F, of the softwood, sw, and hardwood, hw: in a pulp blend using the equations:
Fsw = Csw(Lwm - Lwh) / [ Csw(Lwm - Lwh) + Chw(Lws - Lwm)]
Fhw=1-Fsw

Fiber Wall Thickness: The average Fiber Wall Thickness (FWT) is calculated using the values of fiber width and the measured specimen coarseness.
The FWT histograms and distributions, as a function of fiber length and width, may also be available.

 

SHIVE ANALYSIS SOFTWARE


The combined cross-sectional area of the 3 fluid layers in the FQA cytometric flow cell is 33 mm². Consequently, large cellulose structures, such as shives, can be analyzed.
A published report (Joss et al, Appita J, 2006) found that 3 morphological parameters are required to properly describe a shive: Effective Length, Shive Area and Branch Index. The FQA-360 measures all 3 of these parameters.
Two shives may have the same effective length and area. By measuring the Branch index, it is possible to distinguish shives that are dense and compact from highly branched shives. Usually branched shives pose fewer problems for sheet runnability.
The optional Shive Analysis runs concurrent with the FQA-360 fiber measurements. The Shive Analysis results include the means, variances and distribution histograms for: Effective Length, Shive Area, and Branch Index.

shive

 

VESSEL ELEMENT ANALYSIS SOFTWARE

 

The Vessel Element Analysis runs concurrent with routine FQA-360 testing. The results include the means, variances and distribution histograms for: The Effective Length, Effective Width, L/W aspect ratio and Area.

vessel

 

EXTERNAL FIBER FIBRILLATION SOFTWARE

 

The FQA-360 measures the Degree of External Fiber Fibrillation (%-DEFF) with at least 2 times greater sensitivity than other optical techniques.
This is achieved with the use of circular polarized light which provides a fiber image contrast that is an order of magnitude greater than non-polarized light techniques.
The %-DEFF is the %-difference between the perimeter of the “smooth” fiber and the exterior perimeter of the fibrils. A higher value relates to a more fibrillated cellulose fiber.

 fibrillation

 

FIBER ANALYSIS MEASUREMENTS


Fiber length is reported either as the fiber contour length, L, or the end-to-end (projected) length, ℓ. Fiber Curl is the gradual and continuous curvature of a fiber and is defined by:

Curl Index = (L/ℓ)-1

curl

 

Kink is an abrupt change in the curvature of a fiber and is defined by the modified Kibblewhite's Kink Index. It is the weighted sum of the number Nx, of kinks within a range of "x" kink angles:

Kink Index = [2N(21-45)+3N(46-90)+4N(91-180)] / LTOTAL

 

The test results include means, variances and distribution histograms for:

• Fiber lengths (Ln, Lw, Lww) at ranges up to 15 mm and at a sensitivity of 0.001mm/test.
• Fiber widths and fiber width as a function of length graphs. Measurement sensitivity is < 1 µm/fiber and < 0.1 µm/test
• Curl Index (numeric & length weighted)
• Kink Angle, Kink Index and kinks/mm
• Numeric %-fines and length-weighted with user selected size limits and ranges

A dedicated built-in LCD screen displays results, status and starts test. Individual fiber images are sent to the PC Workstation for analysis and can be stored while performing all the test measurements.

 

OPTIONS AND ACCESSORIES


Options:
• Coarseness, Fiber Wall Thickness & Hwd/Swd Ratio Software
• Shive Analysis Software
• Vessel Element Analysis Software
• Degree of External Fiber Fibrillation (%) Software
• Calibration Check Fiber Kits
• Water Filter Replacement Kits
• Non-polarizing Optics: Used for opaque fibers and some fibers that do not depolarize light. Also, may be used for fiber length measurement according to ISO 16065-2.

 

Accessories:
OpTiBlend: Stand-alone software that uses the data files from the HiRes FQA and FQA-360 to estimate the %-weight content of up to 5 species
• Beaker Carousel (BC) to automatically test up to 6 specimens
• PC Workstation & Excel™

 

Dimensions (including Beaker Carousel accessory)
• 610 mm L x 560 mm W x 760 mm H (24” L x 22” W x 30” H)

Weight (including Beaker Carousel accessory)
• 45 kg (98 lbs)

Connections
PC Workstation:
• Operating with Windows™ 7 or higher and containing:
• At least 8 GB of RAM, 2 ea. Gigabit Ethernet connections, and a USB port, Microsoft Excel™ (2007, 2010 or higher)
• Minimum 20” display is recommended
• Power: 200W stable within 2% and transient free within 10%
• Water: Pressure = 275 kPa (40 PSI) mineral free (less than 50 mg/L residue after evaporation) filtered (external at 5 μm) air-free (less than 0.05% free and bound air by volume)

 

The OpTiBlend (OTB) software estimates the mass ratio of pulp species in an unknown blend. The software can only be used in conjunction with data from the HiRes FQA or FQA-360 [serial number starting with LDA02, LDA12 or LDA17].

 

Ten Important Features for a Fiber Quality Analyzer

 

Whether you are measuring fiber properties in your daily operations, or for research, experience has shown that these are important features to consider when purchasing a fiber quality analyzer.

 

1. Compliance with test methods TAPPI T271, ISO 16065-1, and ISO 16065-2.

 

2. Circular polarized light to provide the highest possible repeatability and most accurate measurement of fiber length and shape. Sample cleaning and de-airing are not necessary since using circular polarized light means air bubbles and contaminants (ink, fillers, extractives, pitch, etc.) are not detected.

 

3. A cytometric flow-cell to orient fibers for correct image analysis and to resist plugging or fouling. Easily measure difficult pulps without special pre-treatment or screening. These fibers include high shive content pulps, mechanical pulps, linerboard pulps, diaper fluff and pulps with high flocculation propensity, recycled fibers, non-wood (plant) fibers, and long synthetic fibers (birefringent such as aramid and collagen).

 

4. The ability to measure fibers that are up to 15mm in length.

 

5. Measure the degree of external fiber fibrillation percentage (DEFF%).

 

6. Measure fiber wall thickness (FWT) when you measure the coarseness with polarized light (ISO 23713).

 

7. The choice to select circular polarized or non-polarized optics (for non-birefringent fibers such as carbon) prior to performing a test.

 

8. Measure up to 6 specimens with a beaker carousel.

 

9. Analyze the shive and vessels elements.

 

10. Determine the hardwood-to-software ratio.

 

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